SDS Volume (819)

Volume 38. Hydrocarbons in Water and Seawater, Part II, p None

Original Measurements

Chernoglazova, F. S.; Simulin, Yu. N.; Zh. Fiz. Khim. 1976, 50, 809.

Variables:

Room Temp: 20 - 70 °C

Prepared by:

Z. Maczynska, A. Maczynski

Method/Apparatus/Procedure:

The solubility of (1) in (2) was determined by the synthetic method of Fuhner [1]. Glass tubes filled with 50-100 mL of (2) were frozen and then (1) was micropipetted. Next, the tubes were sealed and thermostatted for 6 hrs at 70 °C and 72 hrs at 20 °C. The solubility was followed visually. The samples were incremented at regular steps 0.005 g (1)/100 g (2). The mean value from 5-6 determinations was adopted. The solubility of (2) in (1) was determined by gas chromatography. The LKhM-7a instrument equipped with a katharometer was employed.

Source and Purity of Materials:

1. Source not specified; 99.9 purity by glc.
2. Distilled.

Estimated Errors:

Ambient temperature: Not specified.

References

¹ Fühner, H.; Ber. Dtsch. Chem. Ges. 1924, 57, 510-15.