SDS Volume

Volume 20. Halogenated Benzenes, Toluenes and Phenols with Water, p 175

Source Publication

Vesala, A.; Ph.D. Dissertation, University of Turku, Turku, 1973.

Conditions:

Room Temp: 25.0 °C

Compiler:

A.L. Horvath

Methodology:

The solute was equilibrated with water by stirring in a sealed flask [1] with a magnetic stirrer for 48 hours at constant temperature. A sample was withdrawn and filtered through a glass-wool plug and the solute was extracted with 2,2,4-trimethylpentene. The optical densities were determined spectrophotometrically [2]. The mean and standard deviation were obtained from eight independent measurements.

Sample Information:

1. Merck AG., >99% GLC, used as received.
2. Distilled, deionized, and degassed.

Measurement Errors:

Ambient temperature: ±0.05 K.
Mass concentration (m/v) (1): ±1.51%.

Methodology Citations

¹ Franks, F.; Gent, M.; Johnson, H. H.; J. Chem. Soc. 1963, 2716-23.
² Wauchope, R. D.; Getzen, F. W.; J. Chem. Eng. Data 1972, 17(1), 38-41.