SDS Volume (3146)
Volume 67. Halogenated Ethanes and Ethenes with Water, p 517
Original Measurements
Vogel, A. I.; rev. by Furniss, B. S.; et al. Vogel's Textbook of Practical Organic Chemistry, 5th ed. (Longman, London, 1989), p. 1442.
Variables:
Room Temp: 293 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
The solubility determination was carried out in small test tubes (e.g. 100 x 12 mm) to permit vigorous shaking of the solvent and solute mixtures. During the experiment, 0.20 mL 1,1,2,2-tetrachloroethane was added to 3.0 mL of water and agitated concentration of 1,1,2,2-tetrachloroethane in water was analyzed by passing the sample through a chromatographic column.
Source and Purity of Materials:
- Commercial reagent, used as received.
- Distilled.
Estimated Errors:
Ambient temperature: ±1 K (compiler).
Mass concentration (m/v) (1): Not specified.
Components:
- 1,1,2,2-Tetrachloroethane, $\ce{ C2H2C14 }$; [79-34-5] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | 100w1 | $x_{1}$ | $mol_{1}/\pu{100 g}$ (mol/g) |
|---|---|---|---|
| 20.0 | 0.29 | 3.12 x 10-4 | 1.73 x 10-5 |
