SDS Volume

Volume 38. Hydrocarbons in Water and Seawater, Part II, p None

Source Publication

Sutton, C.; Calder, J. A.; Environ. Sci. Technol. 1974, 8, 654-7.

Conditions:

Room Temp: 25 °C

Compiler:

M.C. Haulait-Pirson

Methodology:

175 mg (1) were equilibrated with 700 mL (2) in closed flasks by shaking on a constant temperature bath for 12 hours. The flasks were then allowed to stand for 24 hours. Aliquots of 100 mL were removed, filtered through a 0.45 µm Millipore filter, then extracted three times with 10-mL portions of hexane containing an internal standard. The concentration of (1) was determined by injection of the hexane extract into a dual column gas chromatograph equipped with flame ionization detectors.

Sample Information:

1. Analabs Inc., 99+%
2. doubly distilled.

Measurement Errors:

Ambient temperature: ±0.1°C
Mass concentration (m/v) (1): ±16%