SDS Volume (5230)

Volume 37. Hydrocarbons in Water and Seawater, Part I, p 108

Original Measurements

Booth, H. S.; Everson, H. E.; Ind. Eng. Chem. 1949, 41, 2627-8.

Variables:

Room Temp: 25 and 60 °C

Prepared by:

Z. Maczynska, A. Maczynski

Method/Apparatus/Procedure:

Stoppered Babcock tubes with neck graduated from 0 to 1.6 mL in steps of 0.02 mL were used. A known volume of (2) (generally 50 mL) was added to the tube in a constant temperature water bath and weighed quantities of (1) were added to this solution. Then the mixture was separated by gentle rotation. After this treatment, the volume was determined directly.

Source and Purity of Materials:

1. Source not specified; CP or highest commercial grade ; used as received.
2. Distilled.