SDS Volume (5169)

Volume 78. Acetonitrile Binary Systems, p None

Original Measurements

Sinegubova, S. I.; Ph.D. Dissertation, Saratov University 1978.

Variables:

Room Temp: 298 - 341 $\pu{K}$

Prepared by:

N.V. Sazonov, V.P. Sazonov

Method/Apparatus/Procedure:

The synthetic method was used. Sealed ampoules were placed in a glass-walled thermostat. The temperature of the thermostat was increased gradually with periodic stirring and a preliminary determination of the clear-point temperature in every ampoule was made. A more precise value of the cloud-point temperature was determined by allowing the thermostat to cool. The determination was repeated several times.

Source and Purity of Materials:

1. Source not specified; pure grade product; distilled over anhydrous soda, BP = 81.6°C, $n_{D}^{20}$ = 1.3441, $\rho^{25} = \pu{777 g L-1}$
2. Source not specified; for chromatography; not purified; BP = 36.0°C, $n_{D}^{20}$ = 1.3578, $\rho^{20} = \pu{626 g L-1}$.

Estimated Errors:

Ambient temperature: ±0.2 K.