SDS Volume (5104)

Volume 78. Acetonitrile Binary Systems, p None

Original Measurements

Ralston, A. W.; Hoerr, C. W.; Pool, W. O.; Harwood, H. J.; J. Org. Chem. 9, 102-112 (1944).

Variables:

Room Temp: 253 - 286 $\pu{K}$

Prepared by:

N.V. Sazonov, V.P. Sazonov

Method/Apparatus/Procedure:

The solubility measurements were made with the equipment and in the manner previously described elsewhere [1,2].

Source and Purity of Materials:

1. Source not specified; purity not specified; freshly distilled and cooled without access to the atmosphere, to prevent contamination with carbon dioxide.
2. Prepared by hydrogenation of the highly purified nitrile as in work [1]; purified by two vacuum distillations; FP = 16.11°C

Estimated Errors:

Ambient temperature: Not specified.
Mass concentration (m/v) (1): Not specified

References

¹ Hoerr, C. W.; Binkerd, E. F.; Pool, W. O.; Ralston, A. W.; J. Org. Chem. 9, 68-80 (1944).
² Ralston, A. W.; Hoerr, C. W.; Hoffman, E. J.; J. Am. Chem. Soc. 64, 1516 (1942).