Compilation - Nitroethane with Tridecanoic acid (IUPAC SDS Volume 77)

SDS Volume (4984)

Volume 77. Nitroalkanes with Water or Organic Solvents: Binary and Multicomponent Systems, p None

Original Measurements

Hoerr, C. W.; Ralston, A. W.; J. Org. Chem. 9, 329-37 (1944).

Variables:

Room Temp: 273 - 313 $\pu{K}$

Prepared by:

N.I. Lisov, V.P. Sazonov

Method/Apparatus/Procedure:

The synthetic method, as described in Hoerr, et al. [1], was used. No details were reported.

Source and Purity of Materials:
  1. Source not specified; purity not specified; dried and twice distilled.
  2. Source not specified; purified according to Pool and Ralston [2], FP = 41.76°C.
Estimated Errors:

Ambient temperature: Not specified.
Mass concentration (m/v) (1): Not specified.

References

1 Hoerr, C. W.; Binkerd, E. F.; Pool, W. O.; Ralston, A. W.; J. Org. Chem. 9, 68-80 (1944).
2 Pool, W. O.; Ralston, A. W.; Ind. Eng. Chem. 34, 1104 (1942).

Components:
  1. Nitroethane, $\ce{ C2H5NO2 }$; [79-24-3] NIST WebBook
  2. Tridecanoic acid, $\ce{ C13H26O2 }$; [638-53-9] NIST WebBook
Experimental Data
Solubility of tridecanoic acid (2) in nitroethane (1)
$T$ (°C) $T$ ($\pu{K}$) MR2 (g2/100 g1) 100w2 $x_{2}$
0.0273.2 1.4 1.45 x 10-3
10.0283.2 2.1 2.17 x 10-3
20.0293.2 4.5 4.30.016
30.0303.2 17.3 14.80.057
40.0313.2 9 x 103 98.90.969

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