SDS Volume (4974)

Volume 77. Nitroalkanes with Water or Organic Solvents: Binary and Multicomponent Systems, p None

Original Measurements

Hoerr, C. W.; Ralston, A. W.; J. Org. Chem. 9, 329-37 (1944).

Variables:

Room Temp: 273 - 293 $\pu{K}$

Prepared by:

N.I. Lisov, V.P. Sazonov

Method/Apparatus/Procedure:

The synthetic method, as described in Hoerr, et al. [1], was used. No details were reported.

Source and Purity of Materials:

1. Source not specified; purified according to Hoerr et al. [1]. (dried and twice distilled).
2. Purified according to Pool and Ralston [2]; FP = 28.13°C.

Estimated Errors:

Ambient temperature: Not specified.
Mass concentration (m/v) (1): Not specified.

References

¹ Hoerr, C. W.; Binkerd, E. F.; Pool, W. O.; Ralston, A. W.; J. Org. Chem. 9, 68-80 (1944).
² Pool, W. O.; Ralston, A. W.; Ind. Eng. Chem. 34, 1104 (1942).