SDS Volume (4973)

Volume 77. Nitroalkanes with Water or Organic Solvents: Binary and Multicomponent Systems, p None

Original Measurements

Majgler-Baranowska, H.; Pyzuk, W.; Jeute, W.; Ziolo, J.; J. Chem. Eng. Data 26, 51-3 (1981).

Variables:

Room Temp: 288 - 294 $\pu{K}$

Prepared by:

N.V. Sazonov, V.P. Sazonov

Method/Apparatus/Procedure:

The synthetic method was used. Miscibility temperature was determined by observing turbidity changes during heating and cooling of vigorously shaken solutions. No experimental details given.

Source and Purity of Materials:

1. Fluka; initial purity 95 mass%; purified agitation with sulfuric acid, washing, dried and distilled under reduced pressure over $\ce{CaSO4}$.
2. Source not specified; purity 98 mass%; dried, vacuum fractionated and redistilled over $\ce{CaH2}$.

Estimated Errors:

Ambient temperature: ±0.05 K.

References

¹ Weissberger, A.; Proskauer, E. S.; Riddick, I. A.; Toops, E. E.; Organic Solvents, 2nd ed. (New York, 1995).
² Marsden, C.; Mann, S.; Solvents Guide, Cleaver-Hume Press Ltd., London, 1963.