SDS Volume

Volume 77. Nitroalkanes with Water or Organic Solvents: Binary and Multicomponent Systems, p None

Source Publication

Clever, H. L.; Pirkle Jr., Q. R.; Allen Jr., B. J.; Derrick, M. E.; J. Chem. Eng. Data 17, 31-4 (1972).

Conditions:

Room Temp: 331 $\pu{K}$

Compilers:

N.I. Lisov, V.P. Sazonov

Methodology:

The synthetic method was used. Solution of (1) and (2) were prepared by mass from glass syringes in 13 mm x mm Kimax screw cap culture tubes and sealed with a Teflon-faced rubber liner. Tubes were immersed in a 3 L stirred water bath. Two cloud point observations were made visually; one at relatively fast cooling rate, and the second at a slow cooling rate to more precisely determines cloud point temperature.

Sample Information:

1. Matheson, Coleman and Bell; practical grade; distilled at 57°C/12.9 kPa.
2. Phillips; purity 99 mol%.

Measurement Errors:

Ambient temperature: ±0.1 K.