Compilation - Nitroethane with 1-Nonanol (IUPAC SDS Volume 77)
SDS Volume (4961)
Volume 77. Nitroalkanes with Water or Organic Solvents: Binary and Multicomponent Systems, p None
Original Measurements
Zhuravleva, I. K.; Zhukova, L. M.; Izv. Vyssh. Ucheb. Zaved.; Khim. Khim. Tekhnol. 20, 516-8 (1977).
Variables:
Room Temp: 266 - 290 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
The synthetic method was used. No details were reported.
Source and Purity of Materials:
- Source not specified; distilled; BP = 114°C; $n_{D}^{20}$ = 1.3910, $d_{4}^{20}$ = 1.052.
- Source not specified; distilled; BP = 213°C; MP = 5.3°C; $n_{D}^{20}$ = 1.4310, $d_{4}^{20}$ = 0.828.
Estimated Errors:
Ambient temperature: Not specified.
Mass concentration (m/v) (1): Not specified.
Components:
- Nitroethane, $\ce{ C2H5NO2 }$; [79-24-3] NIST WebBook
- 1-Nonanol, $\ce{ C9H20O }$; [143-08-8] NIST WebBook
Experimental Data
Monotectic equilibrium occurs 265.9 K.
Mutual solubility of nitroethane (1) and 1-nonanol (2)
| $T$ (°C) | $T$ ($\pu{K}$) | 100w1 | $x_{1}$ |
|---|---|---|---|
| -7.0 | 266.2 | 12.5 | 0.215 |
| 0.0 | 273.2 | 16.2 | 0.271 |
| 3.0 | 276.2 | 18.2 | 0.300 |
| 5.0 | 278.2 | 20.2 | 0.327 |
| 10.0 | 283.2 | 24.8 | 0.388 |
| 16.5 | 289.7 | 53.0 | 0.684 |
