SDS Volume

Volume 20. Halogenated Benzenes, Toluenes and Phenols with Water, p 166

Source Publication

Filippov, T. S.; Furman, A. A.; Zh. Prikl. Khim. 1952, 25, 895-7.

Conditions:

Room Temp: 17.7 - 49.0 °C

Compiler:

A.L. Horvath

Methodology:

Measured amounts of water and chlorobenzene were introduced into a tared ampoule which was then sealed. The ampoule was constantly shaken in a thermostat at a series of regulated temperatures until it appeared cloudy. Variations in temperature for clouding and clearing conditions were not more than 0.2-0.3 °C. This procedure for solubility measurements has been referred to as the cloud point method by Alexejew [1].

Sample Information:

1. Double distilled.
2. Source not known, distilled three times over freshly calcined calcium oxide.

Measurement Errors:

Ambient temperature: ±0.1 K (compiler).
Mass concentration (m/v) (1): ±5% (compiler).

Methodology Citation

¹ Alexejew, W.; Ann. Phys. Chem. 28, 305 (1886).