Nitromethane with 2,2’-Iminobisethanol and 1-Pentadecanol (IUPAC SDS Volume 72)

SDS Volume

Volume 72. Nitromethane with Water or Organic Solvents: Ternary and Quaternary Systems, p 1592

Source Publication

Zhuravleva, I. K.; Zhuravlev, E. F.; Mukhametshina, V. B.; Khisametdinova, Z. Z.; Zh. Fiz. Khim. 51, 1003 (1977).

Conditions:

Room Temp: 301 - 348 $\pu{K}$

Compilers:

M.F. Chernysheva, V.P. Sazonov

Methodology:

The synthetic method was used. No experimental details given.

Sample Information:
  1. Source not specified; purity not specified; BP = 101.3°C, $n_{D}^{20}$ = 1.3820, $d_{4}^{20}$ = 1.1320.
  2. Source not specified, purity not specified; MP = 28°C, $n_{D}^{20}$ = 1.4780, $d_{4}^{20}$ = 1.0965.
  3. Source not specified, purity not specified; BP = 162°C/0.067 kPa, BP = 43.0°C, $n_{D}^{50}$, = 1.4390.
Measurement Errors:

Ambient temperature: Not specified.

System Components:
  1. Nitromethane, $\ce{ CH3NO2 }$; [75-52-5] NIST WebBook
  2. 2,2'-Iminobisethanol, $\ce{ C4H11NO2 }$; [111-42-2] NIST WebBook
  3. 1-Pentadecanol, $\ce{ C15H32O }$; [629-76-5] NIST WebBook
Experimental Data

The solubility temperatures of the liquid phases were determined in ternary mixtures with a constant mass relationship of (2) and (3) 20.0:80.0, 30.0:70.0, 40.0:60.0, 50.0:50.0, 60.0:40.0, 70.0:30.0, 80.0:20.0, and 90.0:10.0, respectively.

$T$ (°C) $T$ ($\pu{K}$) w1 w2 $x_{1}$ $x_{2}$
35.0308.2 0.4500.200 0.6820.176
39.0312.2 0.4500.525 0.5910.400
42.0315.2 0.4500.500 0.5970.385
48.5321.7 0.4500.450 0.6100.354
49.0322.2 0.4500.300 0.6510.252
50.0323.2 0.4500.425 0.6160.338
53.0326.2 0.4500.350 0.6370.288
37.0310.2 0.5500.425 0.6850.307
37.5310.7 0.5500.175 0.7590.140
44.0317.2 0.5500.400 0.6910.292
48.0321.2 0.5500.250 0.7350.194
52.0325.2 0.5500.300 0.7200.228
53.0326.2 0.5500.340 0.7080.254
37.5310.7 0.5000.180 0.7250.151
38.0311.2 0.5000.475 0.6390.352
50.5323.7 0.5000.400 0.6590.310
50.5323.7 0.5000.300 0.6870.239
51.0324.2 0.5000.325 0.6800.257
52.5325.7 0.5000.360 0.6700.280

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