SDS Volume

Volume 20. Halogenated Benzenes, Toluenes and Phenols with Water, p 162

Source Publication

Hutchinson, C. A.; Lyon, A. M.; Columbia University Report A-745, July 1, 1943.

Conditions:

Room Temp: 25 °C

Compiler:

A.L. Horvath

Methodology:

Mixtures of 1 to 15 volume ratios of solute to solvent were introduced into an equilibration flask and placed in water thermostat bath. The assembly was shaken mechanically for about 90 minutes at constant temperature. The amount of water in the organic phase was determined by a modified Karl Fischer titration. The determinations were done in triplicate. The experimental procedure was taken from a secondary source [1]. The original report is no longer available.

Sample Information:

1. Distilled.
2. Source is not known, purified and dried before use.

Measurement Errors:

Ambient temperature: ±0.05 K.
Mass concentration (m/v) (1): ±1%.

Methodology Citation

¹ Eidinoff, M. L. In "Production of Heavy Water", National Nuclear Energy Series Division III-Vol. 4F, Murphy, G. M.; Urey, H. C.; Kirshenbaum, I.; Eds.; McGraw-Hill: New York, 1955; Part II, Chapter 7, pp 129-44.