SDS Volume (4386)

Volume 71. Nitromethane with Water or Organic Solvents, p None

Original Measurements

Donahue, D. J.; Bartell, F. E.; J. Phys. Chem. 1952, 56, 480-4.

Variables:

Room Temp: 298 $\pu{K}$

Prepared by:

V.P. Sazonov

Method/Apparatus/Procedure:

Mixtures of (1) and (2) were placed in glass-stoppered flasks and shaken occasionally for 3 d in a water bath. The organic phase was analyzed for water content by the Karl Fischer method. The aqueous phase was analyzed interferometrically.

Source and Purity of Materials:

1. Source not specified; best reagent grade; purified by fractional distillation.
2. distilled.

Estimated Errors:

Ambient temperature: ±0.1 K.