SDS Volume (4326)
Volume 71. Nitromethane with Water or Organic Solvents, p None
Original Measurements
Zhuravleva, I. K.; Zhuravlev, E. F.; Islamova, R. S.; Zh. Fiz. Khim. 48, 1863 (1974).
Variables:
Room Temp: 291 - 339 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
The synthetic method [1] was used. No further details were reported.
Source and Purity of Materials:
- Source not specified; pure grade reagent; freshly distilled.
- Source not specified; pure grade reagent; freshly distilled.
Estimated Errors:
Ambient temperature: Not reported.
Mass concentration (m/v) (1): Not reported.
Pressure: Not reported.
References
1 Alekseev, V. F.; Zh. Russ. Fiz. -Khim. O-va 8, 249 (1876).
Components:
- Nitromethane, $\ce{ CH3NO2 }$; [75-52-5] NIST WebBook
- 2,2'-Iminobisethanol, $\ce{ C4H11NO2 }$; [111-42-2] NIST WebBook
Experimental Data
Mutual solubility of nitromethane and 2,2'-iminobisethanol
| $T$ (°C) | $T$ ($\pu{K}$) | 100w1 | $x_{1}$ |
|---|---|---|---|
| 18.0 | 291.2 | 26.0 | 0.377 |
| 18.0 | 291.2 | 98.5 | 0.991 |
| 30.0 | 303.2 | - | - |
| 30.0 | 303.2 | 98.0 | 0.988 |
| 34.5 | 307.7 | 30.0 | 0.425 |
| 34.5 | 307.7 | - | - |
| 39.2 | 312.4 | - | - |
| 39.2 | 312.4 | 96.7 | 0.981 |
| 43.5 | 316.7 | 33.3 | 0.462 |
| 43.5 | 316.7 | - | - |
| 46.5 | 319.5 | - | - |
| 46.5 | 319.5 | 96.4 | 0.979 |
| 52.5 | 325.7 | - | - |
| 52.5 | 325.7 | 94.2 | 0.966 |
| 58.0 | 331.2 | 42.5 | 0.560 |
| 58.0 | 331.2 | 91.5 | 0.949 |
| 61.0 | 334.2 | - | - |
| 61.0 | 334.2 | 88.3 | 0.929 |
| 61.9 | 335.1 | 50.0 | 0.633 |
| 61.9 | 335.1 | - | - |
| 63.2 | 336.4 | 54.0 | 0.669 |
| 63.2 | 336.4 | - | - |
| 65.0 | 338.2 | - | - |
| 65.0 | 338.2 | 80.0 | 0.873 |
| 65.5 | 338.7 | - | - |
| 65.5 | 338.7 | 73.3 | 0.825 |
| 65.8 | 339.0 | 62.7 | 0.743 |
| 65.8 | 339.0 | - | - |
| 66.0 | 339.2 | 67.5 | 0.782 |
| 66.0 | 339.2 | - | - |
| 68.5 | 341.7 | 68.5 | 0.789 |
| 68.5 | 341.7 | 68.5 | UCST |
