SDS Volume

Volume 71. Nitromethane with Water or Organic Solvents, p 1191

Source Publication

Walden, P.; Z. Phys. Chem. 55U, 683-720 (1906).

Conditions:

Room Temp: 273 and 298 $\pu{K}$

Compiler:

V.P. Sazonov

Methodology:

The analytical method was used.

• Method A: 10 to 20 mL of (1) and an appropriate amount of fine dry salt were placed into a glass retort in a thermostat and stirred for many hours. Aliquots of the saturated solution were taken by pipette for titration.
• Method B: 15-25 mL of (1) and finely divided salt were equilibrated at 40 °C with intensive stirring for one hour. The flask was then placed into a thermostat (25 or 0 °C) and stirred for two hours. After this, stirring was halted and the flask kept at the given temperature for 17-18 hrs. The saturated solutions were then sampled and titrated.

Sample Information:

1. Not specified.
2. Not specified.

Measurement Errors:

Ambient temperature: Not reported.
Mass concentration (m/v) (1): Not reported.
Pressure: Not reported.