Solubility System: Nitromethane with 1-Decanol
Components:

(1) Nitromethane, CH3NO2 ; [75-52-5] NIST WebBook
(2) 1-Decanol , C10H22O; [112-30-1] NIST WebBook

Original Measurements

Sazonov, V. P.; Zh. Obshch. Khim. 59, 2431-5 (1989).

Variables:

Ambient temperature: 298 - 333 K

Prepared by:

N.V. Sazonov, V.P. Sazonov

Method/Apparatus/Procedure:

The synthetic method was used. The apparatus with visual indication of turbidity was described by Sazonov and Chernysheva.1 No further details were reported.

Source and Purity of Materials:
  1. Source not specified; pure grade reagent; fractionally distilled; 99.85 mass% purity; n(20°C,D) = 1.3819, d(20°C) = 1138.0 g L−1.
  2. Source not specified; pure grade reagent;purified by vacuum distillation; 99.3 mass% purity.
Estimated Errors:

Ambient temperature: Not reported.
Mass concentration (m/v) (1): Not reported.
Pressure: Not reported.

References

1 Sazonov, V. P.; Chernysheva, M. F.; Zh. Obshch. Khim. 57, 46-54 (1987).

Experimental Values:
Mutual solubility of nitromethane and 1-decanol
T (°C) T (K) 100w1 x1
25.0 298.2 7.7 1.78 x 10-1
25.0 298.2 96.5 9.86 x 10-1
31.0 304.2 - -
31.0 304.2 95.0 9.80 x 10-1
33.0 306.2 10.1 2.26 x 10-1
33.0 306.2 - -
43.4 316.6 15.0 3.14 x 10-1
43.4 316.6 - -
44.3 317.5 - -
44.3 317.5 90.0 9.59 x 10-1
49.7 322.9 20.0 3.93 x 10-1
49.7 322.9 - -
51.3 324.5 - -
51.3 324.5 85.0 9.36 x 10-1
53.9 327.1 25.0 4.64 x 10-1
53.9 327.1 - -
55.2 328.4 - -
55.2 328.4 79.9 9.12 x 10-1
56.5 329.7 30.0 5.26 x 10-1
56.5 329.7 - -
57.5 330.7 - -
57.5 330.7 75.0 8.86 x 10-1
58.1 331.3 35.0 5.83 x 10-1
58.1 331.3 - -
58.7 331.9 - -
58.7 331.9 70.0 8.58 x 10-1
59.1 332.3 40.0 6.33 x 10-1
59.1 332.3 - -
59.4 322.6 - -
59.4 322.6 65.0 8.28 x 10-1
59.5 332.7 45.0 6.80 x 10-1
59.5 332.7 - -
59.6 332.8 50.0 7.22 x 10-1
59.6 332.8 60.0 7.96 x 10-1
59.7 332.9 55.0 7.60 x 10-1
59.7 332.9 55.0 7.60 x 10-1

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