SDS Volume (4225)

Volume 71. Nitromethane with Water or Organic Solvents, p None

Original Measurements

Sazonov, V. P.; Filippov, V. V.; Izv. Vyssh. Uchebn. Zaved.; Khim. Khim. Tekhnol. 18, 222-5(1975).

Variables:

Room Temp: 293 - 309 $\pu{K}$

Prepared by:

N.V. Sazonov, V.P. Sazonov

Method/Apparatus/Procedure:

The synthetic method of Alekseev was used. Close to the phase transition temperature, heating and cooling of the mixture were accomplished in steps at a rate of 0.02 K/hr.

Source and Purity of Materials:

1. Source not specified; pure grade reagent; distilled through a column of 15 theoretical plates; $n_{D}^{20}$ = 1.3819, $\rho^{20} = \pu{1138.1 g L-1}$.
2. Source not specified; pure grade reagent; distilled through a glass-packed fractionating column; $n_{D}^{20}$ = 1.4182, $\rho^{20} = \pu{819.7 g L-1}$.

Estimated Errors:

Ambient temperature: Not reported.
Mass concentration (m/v) (1): Not reported.
Pressure: Not reported.