SDS Volume (4190)
Volume 71. Nitromethane with Water or Organic Solvents, p None
Original Measurements
Comish, R. E.; Archibald, R. C.; Murphy, E. A.; Evans, H. M.; Ind. Eng. Chem. 26, 397-406 (1934).
Variables:
Room Temp: 314 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
The synthetic method was used. Determinations were made in test tubes, which were heated and allowed to cool slowly in air. Thermometers were roughly calibrated.
Source and Purity of Materials:
- Source not specified; commercial high-grade reagent;
- Source not specified; commercial high-grade reagent.
Estimated Errors:
Ambient temperature: Not reported.
Mass concentration (m/v) (1): Not reported.
Pressure: Not reported.
Components:
- Nitromethane, $\ce{ CH3NO2 }$; [75-52-5] NIST WebBook
- Tetrachloroethene, $\ce{ C2Cl4 }$; [127-18-4] NIST WebBook
Experimental Data
The upper critical solution temperature was reported to be 41°C (314 K, compiler).
