SDS Volume

Volume 71. Nitromethane with Water or Organic Solvents, p None

Source Publication

Schmid, H. H. O.; Mangold, H. K.; Lundberg, W. O.; Microchem. J. 11, 376-83 (1966).

Conditions:

Room Temp: 416 $\pu{K}$

Compiler:

V.P. Sazonov

Methodology:

The synthetic method was used. As described in Schmid, et al. [1], a microscope equipped with a heating stage was used. The sealed glass capillary, containing [1] and (2), was held on the heating stage by an aluminum slide. The stage was cooled by acetone/$\ce{CO2}$, and heated electrically by a regulating transformer. For capillaries with inner diameter 0.2 to 0.3 mm, the amount required for one CST determination is about 0.2 to 2 μL.

Sample Information:

1. Fisher Scientific Co.
2. Not specified.

Measurement Errors:

Ambient temperature: Not reported.
Mass concentration (m/v) (1): Not reported.
Pressure: Not reported.

Methodology Citation

¹ Schmid, H. H. O.; Mangold, H. K.; Lundberg, W. O.; J. Am. Oil Chem. Soc. 42, 372 (1965).