SDS Volume

Volume 69. Ternary Alcohol-Hydrocarbon-Water Systems, p None

Source Publication

Sugi, H.; Katayama, T.; J. Chem. Eng. Jpn. 1977, 10, 400-2.

Conditions:

Room Temp: 298 $\pu{K}$

Compiler:

A. Skrzecz

Methodology:

A combination of titration and analytical method was used. The apparatus and experimental procedure were described in [1]. For GLC analysis a 1.6 m column filled with Poropak-Q was used. Solubility of water in hexane was determined by the Karl Fischer method. Composition of the water-rich phase was determined by the gross composition of phase split liquid mixture and composition of the organic phase (concentration of hexane was assumed to be 0).

Sample Information:

1. Merck Uvasol, spectrograde; used as received; densities agreed within 0.0003 with literature values.
2. Merck Uvasol, spectrograde; used as received; densities agreed within 0.0003 with literature values.
3. De-ionized, twice distilled.

Measurement Errors:

Ambient temperature: Not reported.
Mass concentration (m/v) (1): Not reported.

Methodology Citation

¹ Sugi, H.; Nitta, T.; Katayama, T.; J. Chem. Eng. Jap. 1976, 9, 12.