SDS Volume (3611)

Volume 68. Halogenated Aliphatic Compounds C3-C14 with Water, p None

Original Measurements

Gross, P. M.; Saylor, J. H.; Gorman, M. A.; J. Am. Chem. Soc. 1933, 55(2), 650-2.

Variables:

Room Temp: 298 $\pu{K}$

Prepared by:

A.L. Horvath

Method/Apparatus/Procedure:

The saturated solution was prepared in a flask and placed in a waterbath thermostat. The samples were analyzed using a Zeiss combination liquid and gas interferometer described elsewhere [1]. A detailed description of the complete procedure is given in a MA thesis [2].

Source and Purity of Materials:

1. Eastman Kodak Company, distilled fractionally before use. BP = 120.5-120.6°C.
2. Distilled.

Estimated Errors:

Ambient temperature: ±0.02 K.
Mass concentration (m/v) (1): ±1.0%.

References

¹ Gross, P. M.; Saylor, J. H.; J. Am. Chem. Soc. 1931, 53, 1744-51.
² Gorman, M. A.; M.A. Thesis, Duke University, Durham, NC 1932.