Components:

(1) 3-Bromo-1-propene, C₃H₅Br; [106-95-6] NIST WebBook
(2) Water, H₂O; [7732-18-5] NIST WebBook

Original Measurements

Miller, M. M.; Wasik, S. P.; Huang, G. L.; Shiu, W. Y.; Mackay, D.; Environ. Sci. Technol. 1985, 19, 522-529.

Variables:

Ambient temperature: 298 K

Prepared by:

A.L. Horvath

Method/Apparatus/Procedure:

A saturated aqueous solution was prepared by passing of water through a column which was packed with glass beads coated with 3-bromo-1-propene. The saturated solution was then pumped through an extractor column and 3-bromo-1-propylene was extracted directly into an analytical column. The samples were analyzed with a liquid chromatograph equipped with both an UV absorbance and a fluorescence detector with excitation filters. The peak area was established using a Hewlett-Packard recorder.

Source and Purity of Materials:

1. Eastman Kodak Company, commercial quality, used as received.
2. Double distilled.

Estimated Errors:

Ambient temperature: ±1 K (compiler).
Mass concentration (m/v) (1): Not specified.