SDS Volume

Volume 68. Halogenated Aliphatic Compounds C3-C14 with Water, p None

Source Publication

Vojtko, J.; Hrusovsky, M.; Kanala, A.; Chemicke Zvesti, 21, 443 (1967)

Conditions:

Room Temp: 293 $\pu{K}$

Compiler:

A.L. Horvath

Methodology:

The titration method as described elsewhere [1] was used. Solubility data for the ternary system of water-methanol-2,3-dichloro-1,3-butadiene were also reported.

Sample Information:
  1. Synthesis was described elsewhere [2]. $n_{D}^{20}$ = 1.4887, $d_{4}^{20} = \pu{1.1838 g mL-1}$.
  2. Distilled.
Measurement Errors:

Ambient temperature: ±1.0 K (compiler).
Mass concentration (m/v) (1): Not specified.

Methodology Citations

1 Othmer, D. F.; White, R. E.; Trueger, E.; Ind. Eng. Chem. 1941, 33(10), 1240-8.
2 Carothers, W. H.; Berchett, G. J.; J. Am. Chem. Soc. 55, 2004 (1933).

System Components:
  1. 2,3-Dichloro-1,3-butadiene, $\ce{ C4H4Cl2 }$; [1653-19-6] NIST WebBook
  2. Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
$T$ (°C) w1 100w2 $x_{1}$ $x_{2}$
20 >0.020.02 >3.00.136

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