SDS Volume
Volume 68. Halogenated Aliphatic Compounds C3-C14 with Water, p None
Source Publication
Vojtko, J.; Hrusovsky, M.; Kanala, A.; Chemicke Zvesti, 21, 443 (1967)
Conditions:
Room Temp: 293 $\pu{K}$
Compiler:
Methodology:
The titration method as described elsewhere [1] was used. Solubility data for the ternary system of water-methanol-2,3-dichloro-1,3-butadiene were also reported.
Sample Information:
- Synthesis was described elsewhere [2]. $n_{D}^{20}$ = 1.4887, $d_{4}^{20} = \pu{1.1838 g mL-1}$.
- Distilled.
Measurement Errors:
Ambient temperature: ±1.0 K (compiler).
Mass concentration (m/v) (1): Not specified.
Methodology Citations
1
Othmer, D. F.; White, R. E.; Trueger, E.; Ind. Eng. Chem. 1941, 33(10), 1240-8.
2
Carothers, W. H.; Berchett, G. J.; J. Am. Chem. Soc. 55, 2004 (1933).
System Components:
- 2,3-Dichloro-1,3-butadiene, $\ce{ C4H4Cl2 }$; [1653-19-6] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | w1 | 100w2 | $x_{1}$ | $x_{2}$ |
|---|---|---|---|---|
| 20 | >0.02 | 0.02 | >3.0 | 0.136 |


