Components:

(1) 1,1,2-Trichloro-1,2,2-trifluoroethane, C₂Cl₃F₃; [76-13-1] NIST WebBook
(2) Water, H₂O; [7732-18-5] NIST WebBook

Original Measurements

Howe, G. B.; Mullins, M. E.; Rogers, T. N.; AFESC Tyndall Air Force Base, Report ESL-TR-86-66, Vol. 1, Florida, Sept. 1987, 86 pp. (AD-A188 571).

Variables:

Ambient temperature: 283 - 303 K

Prepared by:

A.L. Horvath

Method/Apparatus/Procedure:

250 cm³ bottles were filled with distilled and deionized water and sealed. Measured volumes of 1,1,2-trichloro-1,2,2-trifluoroethane were injected into the bottles through each bottle septum using a microliter syringe. The solute was in excess of the anticipated solubility limit. The bottles were shaken for 1 hour with a wrist-action shaker and allowed to equilibrate for about three weeks. Samples were then injected into a gas chromatograph equipped with a Carbopack column and a FIDdetector. The gas chromatography (GC) responses were compared with calibration response plots to establish concentrations.

Source and Purity of Materials:

1. Probably a commercial reagent at least 99% purity; used as received.
2. Distilled and deionized.

Estimated Errors:

Ambient temperature: ±0.5 K (compiler).
Mass concentration (m/v) (1): Not specified.