Compilation - 1,2-Dichloroethane with Water (IUPAC SDS Volume 67)
SDS Volume (3309)
Volume 67. Halogenated Ethanes and Ethenes with Water, p 596
Original Measurements
Antropov, L. I.; Populyai, V. E.; Simonov, V. D.; Shamsutdinov, T. M.; Russ. J. Phys. Chem. 1972, 46, 311-2.
Variables:
Room Temp: 291 - 299 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
The Alexejew's synthetic method of solubility determination was used [1]. A fixed weight of 1,2-dichloroethane and water was sealed in a tube and subjected to gradually increasing temperature with constant agitation. The appearance of an opalescence or clouding was an indication of saturation temperature. The temperature was then allowed to fall and an observation made, while the tube was constantly agitated, to establish the temperature of thefirst appearance of opalescence. The observation was repeated several times.
Source and Purity of Materials:
- Source and purity not given.
- Distilled.
Estimated Errors:
Ambient temperature: ±1 K (compiler).
Mass concentration (m/v) (1): Not specified.
References
Components:
- 1,2-Dichloroethane, $\ce{ C2H4Cl2 }$; [107-06-2] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | w1 | 100w2 | $x_{1}$ | $x_{2}$ |
|---|---|---|---|---|
| 18 | - | 0.082 | - | 4.49 x 10-3 |
| 20 | 0.811 | - | 1.49 x 10-3 | - |
| 26 | - | 0.114 | - | 6.23 x 10-3 |
