SDS Volume (3168)

Volume 67. Halogenated Ethanes and Ethenes with Water, p 528

Original Measurements

Coca, J.; Diaz, R. M.; Pazos, C.; Fluid Phase Equilib. 1980, 4, 123-136.

Variables:

Room Temp: 298 $\pu{K}$

Prepared by:

A.L. Horvath

Method/Apparatus/Procedure:

A titration was performed in an Erlenmeyer flask by adding 1,1,1-trichloroethane to water until a permanent turbidity was observed. The flask was immersed in a waterbath thermostat while maintaining a constant agitation using a magnetic stirrer.

Source and Purity of Materials:
  1. Fluka reagent, laboratory grade, further purified by distillation; middle fraction used.
  2. Distilled.
Estimated Errors:

Ambient temperature: ±0.05 K.
Mass concentration (m/v) (1): Not specified.

Components:
  1. 1,1,1-Trichloroethane, $\ce{ C2H3Cl3 }$; [71-55-6] NIST WebBook
  2. Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
$T$ (°C) 100w1 100w2 $x_{1}$ $x_{2}$
25 0.0100.020 1.35 x 10-51.48 x 10-3

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