SDS Volume (3135)

Volume 67. Halogenated Ethanes and Ethenes with Water, p 512

Original Measurements

Chiou, C. T.; Freed, V. H.; "Chemodynamic Studies on Bench Mark Industrial Chemicals"; NTIS: Springfield, VA, 1977; PB-274263.

Variables:

Room Temp: 276 - 307 $\pu{K}$

Prepared by:

A.L. Horvath

Method/Apparatus/Procedure:

An excess of 5-10 g 1,1,2,2-tetrachloroethane was equilibrated with 100 mL of distilled water for 24 hours in a bottle. The aqueous solution taken from the bottle was analyzed using a gas chromatograph equipped with a $\ce{^{63}Ni}$ electron capture detector. The GLC column was packed with porous polymer Chromosorb 101. Further details on determination and evaluation of the procedure are found elsewhere [1].

Source and Purity of Materials:

1. Commercial reagent, used as received.
2. Distilled.

Estimated Errors:

Ambient temperature: ±0.5 K.
Mass concentration (m/v) (1): Not specified.

References

¹ Chiou, C. T.; Schmedding, D. W.; Test. Protoc. Environ. Fate Mov. Toxicants, Proc. Symp., 1980, pp 28-42.