SDS Volume (29)

Volume 20. Halogenated Benzenes, Toluenes and Phenols with Water, p 144

Original Measurements

Jones, J. R.; Monk, C. B.; J. Chem. Soc. 1963, 2633-5.

Variables:

Room Temp: 25 - 35 °C

Prepared by:

A.L. Horvath

Method/Apparatus/Procedure:

Tritiated water was shaken with bromobenzene in 1:10 volume ratios for 4 hours in a flask in a water thermostat bath. The water content was determined by tritium assay. The count rates were determined using a typical liquid scintillator solution technique.

Source and Purity of Materials:

1. Tritiated.
2. Source not known, laboratory grade, dried over CaC $\ce{I2}$ and fractionally distilled before use.

Estimated Errors:

Ambient temperature: ±0.5 K (compiler).
Mass concentration (m/v) (1): ±5%.