SDS Volume

Volume 20. Halogenated Benzenes, Toluenes and Phenols with Water, p 142

Source Publication

Wing, J.; Johnston, W. H.; J. Am. Chem. Soc. 1957, 79(4), 864-5.

Conditions:

Room Temp: 25.0 °C

Compiler:

A.L. Horvath

Methodology:

Tritiated water was equilibrated with 20 mL bromobenzene by stirring in a flask in a constant temperature water bath for two hours. The concentration of the tritiated water in the organic phase was determined by isotopic dilution. The tritium activities in the tritiated water samples were determined by the acetylene method [1,2]. At least four independent experiments were done. The article was based upon work reported in a Ph.D. dissertation [2].

Sample Information:

1. Tracelab, Inc., tritiated water, used as received.
2. Source not specified, chemical grade, redistilled before use.

Measurement Errors:

Ambient temperature: ±0.02 K.
Mass concentration (m/v) (1): ±2.3%.

Methodology Citations

¹ Wing, J.; Johnston, W. H.; Science 1955, 121, 674-5.
² Wing, J.; Ph.D. Dissertation, Purdue University, Lafayette, IN, 1956.