SDS Volume (2513)
Volume 60. Halogenated Methanes with Water, p None
Original Measurements
Zielinski, A. Z.; Chem. Stosowana 1959, 3, 377-84.
Variables:
Room Temp: 298 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
The concentration of water in the organic phase was determined by the Karl Fischer titration method [1].
Source and Purity of Materials:
- Distilled (compiler).
- Gliwice Chemicals, pure grade, used as received.
Estimated Errors:
Ambient temperature: ±1 K (compiler).
Mass concentration (m/v) (1): Not specified.
References
1 Mitchell, J.; Smith, D. M.; Aquametry: A Treatise on Methods for the Determination of Water, Wiley, New York, 1952, p. 73 and 260.
Components:
- Tetrachloromethane, $\ce{ CCl4 }$; [56-23-5] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | ρ (g/L) | 100w1 | $x_{1}$ |
|---|---|---|---|
| 25 | 1.54 | 0.0972 | 8.24 x 10-3 |
