SDS Volume (2509)
Volume 60. Halogenated Methanes with Water, p None
Original Measurements
Eberius, E.; Wasserbestimmung mit Karl-Fischer-Losung (Verlag, GMBH, Weinheim, 1954), p. 67.
Variables:
Room Temp: 293 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
A 50 g tetrachloromethane sample was shaken with pure water in a 100 mL Erlenmeyer flask. The two phases were separated when equilibrium had been established. The organic phase was analyzed for water using the Karl Fischer titration method. Five determinations were performed.
Source and Purity of Materials:
- Distilled.
- Source and purity not given.
Estimated Errors:
Ambient temperature: Not specified.
Mass concentration (m/v) (1): See above.
Components:
- Tetrachloromethane, $\ce{ CCl4 }$; [56-23-5] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | 100w1 | $x_{1}$ | $mol_{1}/\pu{100 g}$ (mol/g) |
|---|---|---|---|
| 20 | 0.012 | 1.02 x 10-3 | 6.66 x 10-6 |
