Compilation - Dichloromethane with Water (IUPAC SDS Volume 60)
SDS Volume (2468)
Volume 60. Halogenated Methanes with Water, p None
Original Measurements
Ohtsuka, K.; Kazama, K.; Sen't Seihin Shohi Kagaku Kaishi 22, 197-201 (1982).
Variables:
Temperature: 298 K
Prepared by:
Method/Apparatus/Procedure:
Water was added gradually to 50 mL dichloromethane in a flask and then lowered into a thermostat bath. The flask was then shaken vigorously until the first cloud (turbidity) appeared. The water content of the sample was determined by the Karl Fischer titration method.
Source and Purity of Materials:
- Distilled (compiler).
- Commercial JIS extra pure reagent, further purified by conventional methods before use.
Experimental Data
Dichloromethane with Water
Components:
(1) Dichloromethane,
$\ce{ CH2Cl2 }$;
[75-09-2]
NIST WebBook
(2) Water,
$\ce{ H2O }$;
[7732-18-5]
NIST WebBook
Experimental Values:
| T (°C) | 100w1a | x1 |
|---|---|---|
| 25.0 | 1.51 x 10-1 | 7.08 x 10-3 |
