SDS Volume (2452)
Volume 60. Halogenated Methanes with Water, p None
Original Measurements
Gross, P. M.; J. Am. Chem. Soc. 1929, 51, 2362-6.
Variables:
Room Temp: 298 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
A weighted amount of tetrachloromethane was mixed with 1000 g water in a bottle and immersed in a water thermostat. The bottle was placed on a shaker until no more droplets of the liquid remained undissolved. The concentration of the tetrachloromethane in water was determined by using a Zeiss water interferometer. One or more samples were syphoned out for the determination of the solubility. The German translation is also published [1].
Source and Purity of Materials:
- Kahlbaum's sulfur-free analytical reagent, used as received.
- distilled.
Estimated Errors:
Ambient temperature: ±0.01 K.
Mass concentration (m/v) (1): ±5%.
References
Components:
- Tetrachloromethane, $\ce{ CCl4 }$; [56-23-5] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | 100w1 | 100w1 | $x_{1}$ |
|---|---|---|---|
| 25 | 0.077 | 0.077 | 9.02 x 10-5 |
