Compilation - Dichloromethane with Water (IUPAC SDS Volume 60)
SDS Volume (2449)
Volume 60. Halogenated Methanes with Water, p None
Original Measurements
Lees, F. P.; Sarram, P.; J. Chem. Eng. Data 1971, 16, 41-4.
Variables:
Temperature: 298 K
Prepared by:
Method/Apparatus/Procedure:
An apparatus containing the mixture of dichloromethane and water was placed in a thermostat bath. The stirring of the mixture was accomplished by using a glass rod rotated by a horseshoe magnet for about 48 hours. The concentration of water in the organic phase was determined by the Karl Fischer titration method.
Source and Purity of Materials:
- Distilled.
- Source not given. Analytical grade, degassed before use.
Experimental Data
Dichloromethane with Water
Components:
(1) Dichloromethane,
$\ce{ CH2Cl2 }$;
[75-09-2]
NIST WebBook
(2) Water,
$\ce{ H2O }$;
[7732-18-5]
NIST WebBook
Experimental Values:
| T (°C) | 100w1 | x1 | 100w1M1-1 (mol/g) |
|---|---|---|---|
| 25.0 | 1.3 x 10-1 | 6.10 x 10-3 | 7.2 x 10-5 |
