SDS Volume (2353)
Volume 60. Halogenated Methanes with Water, p None
Original Measurements
Desnoyer, M.; Dosage de l'Eau dand les Solvants Organiques par Absorption Infra-Rouge et Mesure des Constantes Dielectriques, Centre D'Etudes Nucleaires de Saclay, Report No. 1254, Saclay, France, June 23, 1959.
Variables:
Room Temp: 299 $\pu{K}$
Prepared by:
Method/Apparatus/Procedure:
The saturation of trichloromethane with water took place at room temperature under vigorous stirring. The concentration of water in the organic rich phase was determined by infrared spectrometry.
Source and Purity of Materials:
- Distilled.
- Source not given. Commercial reagent, washed and dried before use.
Estimated Errors:
Ambient temperature: ±0.5 K (compiler).
Mass concentration (m/v) (1): Not specified.
Components:
- Trichloromethane, $\ce{ CHCl3 }$; [67-66-3] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | w1 | $x_{1}$ | $mol_{1}/\pu{100 g}$ (mol/g) |
|---|---|---|---|
| 26 | 8.6 x 10-4 | 5.67 x 10-3 | 4.77 x 10-5 |
