SDS Volume (2248)

Volume 59. Polycyclic Aromatic Hydrocarbons: Binary Non-aqueous Systems, Part II Solutes F-Z, p 64

Original Measurements

Efremov, N. N.; Fikhomirova, A. N.; J. Russ. Phys. Chem. Soc. 1927, 57, 373-390.

Variables:

Room Temp: N/A

Prepared by:

W.E. Acree, Jr.

Method/Apparatus/Procedure:

Experimental details not given in paper.
Determined using a Toshiniwal Melting Point Apparatus equipped with a precision thermometer.

Source and Purity of Materials:
  1. Purity and chemical source were not specific in paper.
  2. Purity and chemical source were not specific in paper.
Estimated Errors:

Ambient temperature: T/K: precision ±0.2 (compiler). x1: ±0.003 (compiler).

Components:
  1. Fluorene, $\ce{ C13H10 }$; [86-73-7] NIST WebBook
  2. 6-Methyl-2,3,4-trinitrophenol, $\ce{ C7H5N3O7 }$; [89793-90-8] NIST WebBook
Experimental Data

Phase equilibrium data not given in cited paper. Authors report formation of a 1:1 fluorene - 6-methyl-2,3,4-trinitrophenol molecular compound. The two eutectic points occur at x1 = 0.190 and T/K = 358.6 and at x1 = 0.751 and T/K = 363.7.

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