Compilation - 1,4-Dichlorobenzene with Water (IUPAC SDS Volume 20)
SDS Volume (209)
Volume 20. Halogenated Benzenes, Toluenes and Phenols with Water, p 101
Original Measurements
Klemenc, A.; Löw, M.; Rec. Trav. Chim. Pays-Bas 1930, 49(4), 629-40.
Variables:
Room Temp: 55 and 60 °C
Prepared by:
Method/Apparatus/Procedure:
The determination of the solubility was based upon volumetric principles applied to the measurement of excess solute in a calibrated apparatus as described by Rex [1].
Source and Purity of Materials:
- Prepared by chlorination of benzene using iodine as catalyst. The preparate was recrystalized several times in ethanol before use, MP = 52.7°C.
- distilled.
Estimated Errors:
Ambient temperature: ±1 K. (compiler).
Mass concentration (m/v) (1): ±10% (compiler).
References
Components:
- 1,4-Dichlorobenzene, $\ce{ C6H4Cl2 }$; [106-46-7] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | $x_{1}$ | MR1 (g/kg) | m1 (mol/kg) |
|---|---|---|---|
| 55 | 1.912 x 10-5 | 0.156 | 1.061 x 10-3 |
| 60 | 1.998 x 10-5 | 0.163 | 1.109 x 10-3 |
(a) Reported.
(b) Calculated by F. W. Getzen.
(c) Calculated by the compiler.
