SDS Volume (2041)

Volume 59. Polycyclic Aromatic Hydrocarbons: Binary Non-aqueous Systems, Part II Solutes F-Z, p None

Original Measurements

Choi, P. B.; McLaughlin, E.; AIChE J. 1983, 29, 150-153.

Variables:

Room Temp: Temperature $\pu{K}$

Prepared by:

W.E. Acree, Jr.

Method/Apparatus/Procedure:

Analytical balance and constant temperature bath.
Mixtures of known composition were sealed in glass ampoules, and placed in a constant temperature bath. Ampoules were slowly rotated at about 0.25 rps, while the bath temperature was increased by 0.1 K every 1,200 seconds. Temperature at which the last trace of solid disappeared was visually determined.

Source and Purity of Materials:

1. 98.67% minimum, Eastman Kodak Company, USA, was purified by column chromatography and recrystallized from toluene before use.
2. Gold Label, Aldrich Chemical Company, Milwaukee, Wisconsin, USA, was used as received.

Estimated Errors:

Ambient temperature: T/K: precision ±0.05. x₁: ±0.0001 (compiler).