SDS Volume
Volume 20. Halogenated Benzenes, Toluenes and Phenols with Water, p 92
Source Publication
Klemenc, A.; Löw, M.; Rec. Trav. Chim. Pays-Bas 1930, 49(4), 629-40.
Conditions:
Room Temp: 20 - 60 °C
Compiler:
Methodology:
The determinations of the solubility was based upon volumetric principles applied to the measurement of excess solute in a calibrated apparatus as described by Rex [1].
Sample Information:
- Kahlbaum reagent, purified by the method of Friedel and Crafts before use.
- distilled.
Measurement Errors:
Ambient temperature: ±1 K. (compiler).
Mass concentration (m/v) (1): ±10% (compiler).
Methodology Citation
System Components:
- 1,3-Dichlorobenzene, $\ce{ C6H4C12 }$; [541-73-1] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | $x_{1}$ | MR1 (g/kg) | m1 (mol/kg) |
|---|---|---|---|
| 20 | 1.360 x 10-5c | 0.111a | 7.550 x 10-4b |
| 25 | 1.507 x 10-5c | 0.123a | 8.366 x 10-4b |
| 30 | 1.716 x 10-5c | 0.140a | 9.522 x 10-4b |
| 35 | 1.838 x 10-5c | 0.150a | 1.020 x 10-3b |
| 40 | 2.047 x 10-5c | 0.167a | 1.136 x 10-3b |
| 45 | 2.169 x 10-5c | 0.177a | 1.204 x 10-3b |
| 55 | 2.402 x 10-5c | 0.196a | 1.333 x 10-3b |
| 60 | 2.463 x 10-5c | 0.201a | 1.367 x 10-3b |
(a) Reported.
(b) Calculated by F. W. Getzen.
(c) Calculated by the compiler.
