Compilation - 1,3-Dibromobenzene with Water (IUPAC SDS Volume 20)
SDS Volume (172)
Volume 20. Halogenated Benzenes, Toluenes and Phenols with Water, p 60
Original Measurements
Hine, J.; Haworth, H. W.; Ramsay, O. B.; J. Am. Chem. Soc. 1963, 85(10), 1473-6.
Variables:
Room Temp: 30 °C
Prepared by:
Method/Apparatus/Procedure:
An excess of 1,3-dibromobenzene was added to a 4 mL of water in an ampoule which was then sealed. The sealed ampoule was rotated in a constant temperature water bath for a week to establish saturation. The 1,3-dibromobenzene solubility was determined by ultraviolet spectrophotometric measurements using a Beckman DU spectrophotometer.
Source and Purity of Materials:
- Eastman Kodak Co., redistilled before use.
- not specified.
Estimated Errors:
Ambient temperature: ±0.1 K.
Mass concentration (m/v) (1): ±5.6% S.D.
Components:
- 1,3-Dibromobenzene, $\ce{ C6H4Br2 }$; [108-36-1] NIST WebBook
- Water, $\ce{ H2O }$; [7732-18-5] NIST WebBook
Experimental Data
| $T$ (°C) | $x_{1}$ | $C_{1}$ (mol/dm3) |
|---|---|---|
| 30 | 5.184 x 10-6 | 2.86 x 10-4 |
(a) Calculated by F. W. Getzen.
(b) Reported.
(c) Calculated by the compiler.
