Valerii P. Sazonov 1 7.80e+01 Ambient temperature 3 7.80 °C 2 3.512e+02 Ambient temperature 4 3.512 $\pu{K}$ 2 1.008e+02 Boiling point 4 1.008 °C 1 1 Solubility, Solubility data series The synthetic method was used. The reagents, about 1 mL of (1) and 1 to 1.5 mL of (2), were placed in tubes and stirred with a thermometer while the tubes were warmed gradually in a bath of water or glycerol. The temperature of disappearance or reappearance of the cloud due to two liquid phases was read three or four times in each direction. If the final position of the interface was not near the middle of the liquid, the volumes of the reagents were adjusted to make it so. The International Union of Pure and Applied Chemistry Francis, A. W.; Ind. Eng. Chem. 36, 1096-104 (1944). paper https://doi.org/10.1021/ie50420a005 75-05-8 1 C2H3N InChI=1S/C2H3N/c1-2-3/h1H3 WEVYAHXRMPXWCK-UHFFFAOYSA-N 41.052 Acetonitrile Source not specified; pure grade reagent. 108-87-2 2 C7H14 InChI=1S/C7H14/c1-7-5-3-2-4-6-7/h7H,2-6H2,1H3 UAEPNZWRGJTJPN-UHFFFAOYSA-N 98.1861 Methylcyclohexane Not specified. Acetonitrile with Methylcyclohexane