Valerii P. Sazonov 1 7.6e+01 Ambient temperature 2 7.6 °C 2 3.49e+02 Ambient temperature 3 3.49 $\pu{K}$ 2 2.92e+02 Ambient temperature 3 2.92 °C 1 1 Solubility, Solubility data series The synthetic method was used. Miscibility was determined in a glass-stoppered tube of 4 mm inside diameter. Equal volumes (0.1 mL) of (1) and (2) were measured into the tube which was then strapped to a thermometer, warmed to 5 or 10 °C above the solubility temperature, mixed well by shaking, and then allowed to cool slowly, still shaking, in a bath of white oil (above 30 °C), water (below 30 °C), or nonfreezing mixture (below 0 °C). The International Union of Pure and Applied Chemistry Mulliken, S. P.; Wakeman, R. L.; Recl. Trav. Chim. Pays-Bas, 54, 366-72 (1935). paper https://doi.org/10.1002/recl.19350540508 75-52-5 1 CH3NO2 InChI=1S/CH3NO2/c1-2(3)4/h1H3 LYGJENNIWJXYER-UHFFFAOYSA-N 61.04 Nitromethane Not specified. 1079-71-6 2 C14H18 InChI=1S/C14H18/c1-2-6-12-10-14-8-4-3-7-13(14)9-11(12)5-1/h1-2,5,9,12,14H,3-4,6-8,10H2 VTIBBOHXBURHMD-UHFFFAOYSA-N 186.29 Octahydroanthracene Some aromatic hydrocarbons(*) obtained from Mr. J. B. Conant, Harvard University; others were purest commercial samples. Nitromethane with Octahydroanthracene