Valerii P. Sazonov 0 4e+00 Ambient temperature 1 4 °C 2 2.77e+02 Ambient temperature 3 2.77 $\pu{K}$ 2 1.82e+02 Ambient temperature 3 1.82 °C 1 1 Solubility, Solubility data series The synthetic method was used. Miscibility was determined in a glass-stoppered tube of 4 mm inside diameter. Equal volumes (0.1 mL) of (1) and (2) were measured into the tube which was then strapped to a thermometer, warmed to 5 or 10 °C above the solubility temperature, mixed well by shaking, and then allowed to cool slowly, still shaking, in a bath of white oil (above 30 °C), water (below 30 °C), or nonfreezing mixture (below 0 °C). The International Union of Pure and Applied Chemistry Mulliken, S. P.; Wakeman, R. L.; Recl. Trav. Chim. Pays-Bas, 54, 366-72 (1935). paper https://doi.org/10.1002/recl.19350540508 75-52-5 1 CH3NO2 InChI=1S/CH3NO2/c1-2(3)4/h1H3 LYGJENNIWJXYER-UHFFFAOYSA-N 61.04 Nitromethane Not specified. 104-51-8 2 C10H14 InChI=1S/C10H14/c1-2-3-7-10-8-5-4-6-9-10/h4-6,8-9H,2-3,7H2,1H3 OCKPCBLVNKHBMX-UHFFFAOYSA-N 134.218 Butylbenzene Some aromatic hydrocarbons(*) obtained from Mr. J. B. Conant, Harvard University; others were purest commercial samples. Nitromethane with Butylbenzene