Valerii P. Sazonov 1 2.4e+01 Ambient temperature 2 2.4 °C 2 2.97e+02 Ambient temperature 3 2.97 $\pu{K}$ Boiling point °C 105.3-106.7 1 1 Solubility, Solubility data series The synthetic method was used. Miscibility was determined in a glass-stoppered tube of 4 mm inside diameter. Equal volumes (0.1 mL) of (1) and (2) were measured into the tube which was then strapped to a thermometer, warmed to 5 or 10 °C above the solubility temperature, mixed well by shaking, and then allowed to cool slowly, still shaking, in a bath of white oil (above 30 °C), water (below 30 °C), or nonfreezing mixture ( below 0 °C). The International Union of Pure and Applied Chemistry Mulliken, S. P.; Wakeman, R. L.; Recl. Trav. Chim. Pays-Bas, 54, 366-72 (1935). paper https://doi.org/10.1002/recl.19350540508 75-52-5 1 CH3NO2 InChI=1S/CH3NO2/c1-2(3)4/h1H3 LYGJENNIWJXYER-UHFFFAOYSA-N 61.04 Nitromethane Not specified. 2586-89-2 2 C7H12 InChI=1S/C7H12/c1-3-5-7-6-4-2/h3-5H2,1-2H3 KLYHSJRCIZOUHE-UHFFFAOYSA-N 96.17 3-Heptyne 1-hexadecyne synthesized in the Research Laboratory of Organic Chemistry, Massachusetts Institute of Technology; others alkynes were purest commercial samples available from the British Drug Houses. Nitromethane with 3-Heptyne