Valerii P. Sazonov 1 7.5e+01 Ambient temperature 2 7.5 °C 2 3.48e+02 Ambient temperature 3 3.48 $\pu{K}$ 1 2 1.54e+02 Boiling point 3 1.542 °C 1 Solubility, Solubility data series The synthetic method was used. Miscibility was determined in a glass-stoppered tube of 4 mm inside diameter. Equal volumes (0.1mL) of (1) and (2) were measured into the tube which was then strapped to a thermometer, warmed to 5 or 10 °C above the solubility temperature, mixed well by shaking, and then allowed to cool slowly, still shaking, in a bath of white oil. The International Union of Pure and Applied Chemistry Mulliken, S. P.; Wakeman, R. L.; Recl. Trav. Chim. Pays-Bas, 54, 366-72 (1935). paper https://doi.org/10.1002/recl.19350540508 75-52-5 1 CH3NO2 InChI=1S/CH3NO2/c1-2(3)4/h1H3 LYGJENNIWJXYER-UHFFFAOYSA-N 61.04 Nitromethane Not specified. 2157-18-8 2 C9H16 InChI=1S/C9H16/c1-8(2)9-6-4-3-5-7-9/h9H,1,3-7H2,2H3 SWLGTNLRTUGMHV-UHFFFAOYSA-N 124.22 (1-Methylethenyl)cyclohexane (1-methylethenyl)cyclohexane synthesized in the Research Laboratory of Organic Chemistry, Massachusetts Institute of Technology; other cycloalkenes were purest available commercial samples. Nitromethane with (1-Methylethenyl)cyclohexane