Valerii P. Sazonov 0 -2e+00 Ambient temperature 1 -2 °C 2 2.71e+02 Ambient temperature 3 2.71 $\pu{K}$ 2 2.64e+02 Ambient temperature 3 2.64 °C 1 1 Solubility, Solubility data series The synthetic method was used. The reagents, about 1 mL of (1) and 1 to 1.5 mL of (2), were introduced and stirred with a thermometer while the tubes were warmed gradually in a bath of water. The temperature of disappearance or reappearance of the cloud due to two liquid phases was read three or four times in each direction. If the final position of the interface was not near the middle of the liquid, the volumes of the reagents were adjusted to make it so. The International Union of Pure and Applied Chemistry Francis, A. W.; Ind. Eng. Chem. 36, 1096-104 (1944). paper https://doi.org/10.1021/ie50420a005 75-52-5 1 CH3NO2 InChI=1S/CH3NO2/c1-2(3)4/h1H3 LYGJENNIWJXYER-UHFFFAOYSA-N 61.04 Nitromethane Source not specified, pure grade reagent. 6158-45-8 2 C13H14 InChI=1S/C13H14/c1-10(2)12-9-5-7-11-6-3-4-8-13(11)12/h3-10H,1-2H3 PMPBFICDXLLSRM-UHFFFAOYSA-N 170.25 1-propan-2-ylnaphthalene Some aromatic hydrocarbons (*) were available from the Socony-Vacuum Oil Co.; others were made by alkylation of benzene, toluene, ethylbenzene, naphthalene or tetralin with ethene, propene, 2-butene, isobutene or pentene, using aluminum chloride as catalyst. Nitromethane with 1-propan-2-ylnaphthalene