Valerii P. Sazonov 1 8.8e+01 Ambient temperature 2 8.8 °C 2 3.61e+02 Ambient temperature 3 3.61 $\pu{K}$ Boiling point °C 128.7-129.5 1 1 Solubility, Solubility data series The synthetic method was used. Miscibility was determined in a glass-stoppered tube of 4 mm inside diameter. Equal volumes (0.1 mL) of (1) and (2) were measured into the tube which was then strapped to a thermometer, warmed to 5 or 10 °C above the solubility temperature, mixed well by shaking, and then allowed to cool slowly, still shaking, in a bath of white oil (above 30 °C) or water (below 30 °C). The International Union of Pure and Applied Chemistry Mulliken, S. P.; Wakeman, R. L.; Recl. Trav. Chim. Pays-Bas, 54, 366-72 (1935). paper https://doi.org/10.1002/recl.19350540508 75-52-5 1 CH3NO2 InChI=1S/CH3NO2/c1-2(3)4/h1H3 LYGJENNIWJXYER-UHFFFAOYSA-N 61.04 Nitromethane Not specified. 55702-61-9 2 C9H18 InChI=1S/C9H18/c1-6-7-8(2)9(3,4)5/h6-8H,1-5H3 VBQNXPUFZFWMCZ-UHFFFAOYSA-N 126.24 4,5,5-Trimethyl-2-hexene 2-pentene synthesized in the Research Lab of Organic Chemistry Massachusetts Institute of Technology; some alkenes (*) were obtained from Dr. H. E. Buc, Standard Oil Development Co.; the others were the purest commercial samples available from BDH. Nitromethane with 4,5,5-Trimethyl-2-hexene